@lantau: Did you get a chance to use the kit?
Raghu,
I decided not to let 2020 pass without playing with my Scala kit. I had to deliver some shopping items to my brothers famliy, who are in self quarantine. He testest positive, without symptoms, just before the holidays, but no symptoms. I and my other brother, who had direct contact, tested negative after the holidays. So no need to worry. But I took the opportunity in favourable weather to expose the last 17 frames, which came off my bulk roll of Silvermax/Scala 160. Also in the fridge I had a roll of Scala160 with identically exposed frames of a colour checker and a Fuji motion pictures test chart. This roll must have been in the fridge since Summer 2019, because I certainly didn't do it this Summer.
So todays roll of 17 and a part of the roll of identical test images went into the Jobo tank. My Scala 160 needs to be developed at 24°C. Scala 50 at 20°C. The instructions don't really say if the following steps need to be done at 24°C as sell. It does say that the rinse/wash water should be at 20°C +/- 2°.
I used my Cinestill TCS1000 (a sous vide unit, really) to get a waterbath to 24°C and used the opportunity to compare this units internal thermometer with my Kaiser precision capillary thermometer (0.2°C step scale) and the thermometer function of my (not that cheap) Greissinger pH meter, using the attached Pt1000 probe. The TCS is ahead of the Kaiser by 0.2°C and the Greissinger pH Meter is trailing the Kaiser by 0.1°C. All at a nominal 24°C. I'll look at C41 temperature at some other time.
So I did that and had dinner while the TCS1000 was humming along and eventually started the Scala process before it was getting to late on this New Years Eve. And apparently I was a bit too absent minded when I took a bottle out of the water bath and started pouring it into the tank. Turned out to be the bleach. My autopilot really thought the left bottle was the developer and ignored the dark colour of the bottle (purple permanganate bleach in a 250mL brown glass bottle). My brains higher functions kicked in again as it saw the purple liquid pouring into my tank and instinctively poured it back and immediately filled the tank with water.
Oh well. The final fare well of 2020... I immediately had to think of the SLIMT technique. I read about it, but it is a bit further down on my Have-To-Try-It-Out list. After a wash with the Jobo cascade I finally started the first development. Went through the whole process. Slipped to the left in the table with the times and bleached only for 4 Minutes (Scala 50) instead of 6 (Scala 160). No, I had no alcohol at the time!. But caught the error in time, did an extra wash and added two more minutes of bleach time...
Eventually all was done and in general the process works. But pouring out that bleach you can imagine that the film in the spiral was immersed in the bleach on one side. And I do see a sinus curve of higher density come up on the film strip, corresponding to one side of the film spiral. Yes, a few frames damaged. Others are fine. Had I done what you should do to recover from an accident like that, fill the tank with water and then drain, I think I would have created a higher base fog.
So now that you suffered through my New Years Eve adventures (are you still with me?) here comes the part you care about:
- The images look neutral black to me. Not warm. In the coming days I will do digital repro on my copy stand and try to adjust the result to correspond to the real slide. My screens are profiled (it's been a while and a recent hardware rebuild in between, and I may have to reprofile first), which means it will be up to you on your end to have a suitable viewing device that can reproduce a somewhat colour correct image file in a meaningful way.
- I gifted a Heiland b/w densitometer to myself for Xmas. Measuring the base fog of the film (zeroing the device against air) I'm getting a density of 0.09. That is the part of the film that is exposed to ambient light when loading the camera.
- Zeroing the densitometer to the clear film base I got a Dmax (over base fog) at the completely unexposed part of the films lead in of 2.15-2.17. Interesting is, that the bleach has reach parts of that area as well and managed to increase the resulting Dmax to about 2.40 (not uniform). Maybe there is a slight aging of the film (Silvermax was made many years ago) and the bleach removed the latent fog, or maybe that is another effect.
- I did put another Scala 160 under the densitometer. That one was developed in the original Agfa Scala process by Photostudio 13 in Stuttgart. I don't have the clear beginning of the film left, only a Dmax piece as part of the first strip. The lab returns the complete film, including the parts with the marks from the film clips. But I usually throw away the very ends. Zeroing the sensitometer against air again I'm reading an absolute density of 2.50ish (+/- 0.03 depending on where I measure). I measured a clear part of the film (bright, blown out sky) at 0.07. You may want to accept that as base+fog.
I'm finally going to take my first sleep of the year now...