If you purchased the Pyrocat in a glycol kit from Formulary, or mixed it yourself in glycol, there is no way it would have gone bad in a couple of months. In fact, it is good for several years mixed in the glycol kit. To go bad in such a short period of time it would have to have been either improperly mixed, or contaminated.
If you have any sodium carbonate on hand you might prepare a 20% stock solution and use it at 5X the amount of the 75% potassium carbonate stock solution. This should indicate at least if Stock A is good or bad.
Sandy King
I have to agree with those who say you really can't judge your contrast results without printing the negs on photographic paper--ideally the paper you plan to use for the final print--even if you've used other pyro developers, because the visible color of the stain isn't the same for all pyro developers. I wouldn't do any further testing without making some proofs. Even if the proofs confirm your intuitions based on inspection of the negs, that will tell you something.
This sounds similar to a problem I had last year with efke 25 in 4x5 sheets. I bought a box of it and could not for the life of me get contrast, with either rodinal or pyrocat. I eventually returned the box and get a new one that easily built contrast. The problem was with the film, not the developer. There was a problem with the batch apparently.
dude have you read what those with experience have been saying? did you try some of the times given?
Something is very wrong - I can tell from looking at the negatives there is almost no contrast difference. I can tell from my scan that there is no contrast.
I am not even going to bother to print these on general run of the mill Ilford VC.
RB
"Dude" - I don't do stand development so those times do not compute and guess what else dude, If my times/temps were not so far and above ANY of the non-stand development times ANYONE listed AND so far out of any film I have ever experienced using Pyrocat AND I didn't get similar results souping the film in a MUCH MORE ACTIVE developer last night, do you think I would be asking this stuff/complaining?
Well - I wouldn't. I am not the kind of darkroom worker that soups a film one time with no process control without trying a lot of other stuff before I go crying that it doesn't work. I am now 90% sure I have a bad batch of PL 100.
RB
your probably correct in assuming your film is bad given all the testing you have done. I've probably gone through 20 boxes of the stuff and never had a problem. But then again I've had bad boxes from other more prominent manufacturers.
You say you "don't do stand development". Well maybe you should give it a try. It seems to work for the rest of us. I never did as well until I started using PL100.
One question on the stand dev thing - My cursory understanding is that it is used to compensate for the highlights while building contrast in the lows and mids?
I can only echo mentioned bad experiences with EFKE PL100 (AKA MACO UP100) 4*5 film, no matter what I tried I could not build up satisfying density and nice mid ton separation, even stand development in PyrocatMC for 2 hours did not help..I have to conclude I have one of these infamous batches (they were given to me for free by said firm, I now wonder why..;-)..)
Did you try Ilford or Kodak film in your Pyrocat brew?
best,
Cor
The issue I am having that I am convinced is a bad box of PL100 is that it gets to a certain density level let's call it mid-tone level and that is it no matter what you do it stays about there so there is NO density in the highlights it almost like a severe N- exposure/development where you expose the film like crazy and then under develop like crazy - except I didn't and sheets of know good film taken at the same time are fine.
RB
Is there any possibility the film has been fogged? This might explain the problem.
Sandy King
Here is how I would evaluate the film: run a few tests through DK-50 either straight or 1:1. If these come out flat you definitely have bad film. The result for either dilution @ 5mins should be a nice 'punchy' negative.
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