I mixed 100ml of Ferric Oxalate last night and today a sediment has settled at the bottom. I have been making kallitypes for a few years now but never had this happen before. Has some thing gone wrong? Do you simply shake the bottle before use?
I can't say what the sediment is, but maybe it's just undissolved oxalate. Were it me, I wouldn't shake it up. I would, however, try making some prints with it. If it works, I'd just use it as is.
I had some Ferric Oxalate from Nymoc in Toronto several years ago (out of business) that was a real bitch to get into solution. There was always a thick sediment on the bottom. I warmed up the solution, reshook the bottle, and it eventually would dissolve. For years now I've been using FO from B&S. Goes into solution way more easily.