Many thanks for the tips what could have gone wrong.
Here is what I did: I took a series of 4 shots of the same scene for a personal EI for fomapan 100 4x5.
I took my meter reading from the shadow area I want to render as Zone III.
I took my shots carefully, checking all settings etc, changing from ISO 100 to ISO 50 with each shot.
So far so good.
I marked all the negatives before developing by cutting of a corner of each negative according to which number of shot it was, i.e. one corner for the first shot, two corners for the second shot etc, so that I could easily identify them later. I then put the negatives insight of an old 4x5 negative box and the box inside an old black back to protect them from the light, while I set up my chemicals etc.
To develop my negatives I use home-made PVC tubes (1.5 inches in diameter), black ones used for plumbing which I bought in a DIY shop and cut to 5 inch in length.
The tubes are open and the negatives are inserted into the tubes in total darkness and then the tubes go into and old Durst Codrum paper daylight development drum, which takes 3 tubes at a time.
This is the first time I did develop this way. I used the tray method before, but I wanted to try a method to develop in daylight.
The first 3 negatives that I developed (R09 at 1:50 for 7 Minutes) where shot no 1, no 3 and no 4. There is no reason to it, just the way I took them out of the film box.
These negatives developed okay, as I said already, they developed as expected.
When I insert the negatives into the tubes I feel for the notch, make sure it is in the upper right corner and then curl the negatives to fit into the tube, emulsion side up.
The next negatives I developed were shot no 2 and a blank negative.
Here no 2 shot was almost clear with just the faint 'positive' looking image and the blank negative was clear (as expected).
I wonder now as chazzy said, whether I had a lapse of concentration and inserted this negative the wrong way into the tube.
Anyway I learned something new, many thanks for all your answers.