I got a sealed can of Kodak Linagraph pan, expired 1960, pretty positive it was still factory sealed. I am testing short rolls of film for EV. Both of my tests so far have come out with negatives so dark they look totally black from 2-3 feet away (from a few inches they're not nearly so bad). I fixed for 4-5 minutes in the tank. Each time I also tore off a scrap of leader and put it in some of the very same batch of fixer that I developed the film in, and the leader cleared in about 1 minute. I am baffled. The only difference between the leader test and the film in the tank is that one went through developer and the other skipped the developing process (R09 1:100 stand) - is the developer affecting the old film so it doesn't fix? Even the sprocket edges of the film out of the tank is dark, without clearing.